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1 article(s) from Hoossen, Zakiena

Inclusion complexes of the steroid hormones 17β-estradiol and progesterone with β- and γ-cyclodextrin hosts: syntheses, X-ray structures, thermal analyses and API solubility enhancements

Alexios I. Vicatos,
Zakiena Hoossen and
Mino R. Caira

Beilstein J. Org. Chem. 2022, 18, 1749–1762, doi:10.3762/bjoc.18.184

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Graphical Abstract

Figure 1: Chemical structures of 17β-estradiol (top) and progesterone (bottom).

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Figure 2: The PXRD patterns of the β-CD·PRO complex produced via kneading (2:1), an isostructural β-CD comple...

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Figure 3: The PXRD patterns of the γ-CD·PRO complex produced via kneading (3:2), an isostructural γ-CD comple...

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Figure 4: (a) The crystal morphology of β-CD·BES recorded with polarised light. (b) The crystal morphology of...

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Figure 5: (a) A representative DSC curve (n = 2) of β-CD·BES, with the respective TGA curve (n = 3); (b) a re...

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Figure 6: Stereoscopic views of the host molecule and water oxygen atoms in the ASUs of (a) β-CD·BES and (b) ...

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Figure 7: A stereoscopic view down the c-axis displaying the packing arrangement for β-CD·BES.

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Figure 8: A stereoscopic view down the c-axis displaying the packing arrangement for β-CD·PRO.

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Figure 9: A stereoscopic view of the host atoms and water oxygen atoms in the ASU of γ-CD·PRO.

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Figure 10: The host atoms and water oxygen atoms of the ASU viewed down the c-axis, showing that the water mol...

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Figure 11: The distinct packing arrangement of the repeat unit of the host molecules in γ-CD·PRO. The four-fol...

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Figure 12: A stereoscopic view of γ-CD·PRO viewed down the c-axis, which displays the infinite channel packing...

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Published 22 Dec 2022

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